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Anion-exchange separation of Pt and Pd using perchloric and hydrochloric acid solutions

January 1, 1982

On Biorad Ag-1X8 anion-exchange resin (200-400 mesh), Pd and Pt may be separated from one another by elution with 0.2M HClO4, and 5M HClO4, respectively. If present, Au may be retained by making the elutriants 0.003M in HCl. Alternatively, reduction by H2SO3 enables elution of Pt2+ with 6M HCl before recovery of Pd2+ with 0.2M HClO4??Ir4+ is reduced to Ir3+ by H2SO3 and may be eluted ahead of Pt2+ by 2M HCl. ?? 1982 Akade??miai Kiado??.

Publication Year 1982
Title Anion-exchange separation of Pt and Pd using perchloric and hydrochloric acid solutions
DOI 10.1007/BF02520354
Authors R.K. Petrie, J. W. Morgan
Publication Type Article
Publication Subtype Journal Article
Series Title Journal of Radioanalytical Chemistry
Index ID 70000681
Record Source USGS Publications Warehouse