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Capabilities

Organic Geochemistry Research Laboratory (OGRL)

Central Plains Water Science Center, Lawrence, KS

FY 2026 Services

Environmental Organic Chemistry (EOC) Unit

For additional information contact: Julie Dietze 785-832-3564, juliec@usgs.gov or

GS-W-KS_OGRL_EOC@usgs.gov

 

  • All internal Quality Control data must be requested during the establishment of the laboratory work agreement or additional fees may apply.
  • Requested spikes are assessed at the same price per sample as environmental samples.
  • Samples submitted and then later requested not to be analyzed must be submitted in email within 3 days of sample submission or the sample will be assessed analysis costs.
  • Re-analysis requests must be provided within 30 days of data delivery.
  • Original sample bottles will be disposed 12 months after delivery of data unless otherwise agreed upon in the established laboratory work agreement.
  • The OGRL must be notified by the end of Quarter 3 of the current fiscal year of any changes to the estimated sample totals in the established laboratory work agreement or additional fees may apply.  

 

Routine Methods 

Analysis Code:  LCGY

Glyphosate, AMPA, and Glufosinate Method

Sample Prep: Derivatization (FMOC)

Instrumentation: Liquid chromatography/tandem mass spectrometry

Matrix: Water 

Reporting Limit: 0.02 µg/L 

OGRL Method Code: LCM57

Bottle Requirements: 1-20mL VOA amber borosilicate glass vial (filled ½ full) or 1-4oz (125mL) amber glass with Teflon lined caps (filled ½ full). 

Compound Name/ CAS#: Parameter Code 

 

Glyphosate/ 1071-83-6: 62722

*Aminomethylphosphonic Acid (AMPA)/ 1066-51-9: 62649Glufosinate/ 51276-47-2: 62721

Analysis Code:  LCAZ

Atrazine Method

Instrumentation: Direct inject liquid chromatography/tandem mass spectrometry

Matrix: Water

Reporting Limit: 0.05 µg/L 

OGRL Method Code: LM127

Bottle Requirements: 1- 4oz (125mL) amber glass with Teflon lined caps (filled ½ full)

 

Compound/CAS#: Parameter Code

Atrazine/ 1912249: 39632

 

Methods for Tire Wear Particle Chemicals

Analysis Code:  LCTR

Direct Inject Water Method

Instrumentation: Liquid chromatography/tandem mass spectrometry

Matrix: Water

Reporting Limit: 2.0 µg/L 

OGRL Method Code: LM129

Bottle Requirements: Contact Rachael Lane (785-760-4540; rflane@usgs.gov) for details about bottles or additional tire wear compounds of interest 

 

Compound/CAS#: Parameter Code

6PPD-quinone / 2754428-18-5, 39944

6PPD/ 793-24-8, 39945

Other tire-related compounds available by request

 

Analysis Code:  LCTR-EPA

EPA Draft Method 1634

Sample Prep: Solid-phase extraction  

Instrumentation: Liquid chromatography/tandem mass spectrometry

Matrix: Water (predominantly stormwater and surface water)

Reporting Limit: 0.200 ng/L 

OGRL Method Code: LM128

Bottle Requirements: Contact Rachael Lane (785-760-4540; rflane@usgs.gov) for details about bottles or additional tire wear compounds of interest 

 

Compound/CAS#: Parameter Code

6PPD-quinone / 2754428-18-5, 39943

Analysis Code:  LCAB

Four Class Antibiotic Method

Sample Prep: Solid-phase extraction              

Instrumentation: Liquid chromatography/tandem mass spectrometry

Matrix: Water 

Reporting Limit: 0.005 µg/L (except where noted)

Method Notes: 

The concentrations for the family of isomers for chlortetracycline, oxytetracycline, and tetracycline are processed with the following differences and assumptions:

  1. Only one isomer per family is physically added in the standard mix and standard addition solutions (isochlotetracycline, oxytetracycline, tetracycline)
  2. Equal instrument response for each isomer in a family is assumed
  3. Concentration is calculated on the sum of all isomers in a family and proportioned by area of individual isomer

Bottle Requirements: 1-4oz (125mL) amber glass with Teflon lined caps 

 

Compound Name/ CAS#: Parameter Code, Method Code

Fluoroquinolines

Ciprofloxacin/85721-33-1: 62898, LCM48

Enrofloxacin/ 93106-60-6: 66495 LCM48

Lomefloxacin/ 98079-51-7: 62900, LCM48

Norfloxacin/ 70458-96-7: 62757, LCM48

Ofloxacin/ 82419-36-1: 62899, LCM48

Sarafloxacin/ 98105-99-8: 62771, LCM48

Macrolides

Azithromycin/ 83905-01-5: 62792, LCM94

Erythromycin (0.01 µg/L)/ 114-07-8: 62797, LCM95

*Erythromycin-H2O (0.02 µg/L)/ 23893-13-2: 63674, LCM95

Roxithromycin/ 80214-83-1: 62895, LCM48

Tylosin (0.01 µg/L)/ 1401-69-0: 62896, LCM95

Virginiamycin/ 11006-76-1: 62897, LCM48

Sulfonamides

Sulfachloropyridazine/ 80-32-0: 62774, LCM48

Sulfadiazine (0.05 µg/L)/ 68-35-9: 62963, LCM95

Sulfadimethoxine/ 122-11-2: 62776, LCM48

Sulfamethoxazole/ 723-46-6: 62775, LCM48

Sulfamethazine/ 57-68-1: 61762, LCM48

Sulfathiazole (0.05 µg/L)/ 72-14-0: 62778, LCM95

Tetracyclines

Chlortetracycline (0.01 µg/L)/ 57-62-5: 61744: LCM95

*Epi-chlortetracycline (0.01 µg/L)/ 101342-45-4: 63731, LCM95

*Epi-iso-chlortetracycline (0.01 µg/L)/ N/A: 64047, LCM95

*Iso-chlortetracycline/ 514-53-4: 64175, LCM94

Oxytetracycline/ 79-57-2: 61759, LCM94

*Epi-oxytetracycline (0.01 µg/L)/ 35259-39-3: 63729, LCM95

Tetracycline/ 60-54-8: 62781, LCM94

*Epi-tetracycline (0.01 µg/L)/ 79-85-6: 63727, LCM95

Doxycycline (0.01 µg/L)/ 564-25-0: 62694, LCM95

Pharmaceuticals

Carbamazepine/ 298-46-4: 62793, LCM48

Ibuprofen (0.05 µg/L)/ 15687-27-1: 62014, LCM95

Others

Chloramphenicol (0.01 µg/L)/ 56-75-7: 65194, LCM95

Lincomycin/ 154-21-2: 62894, LCM48

Ormetoprim/ 6981-18-6: 62962, LCM48

Trimethoprim/ 738-70-5: 62023, LCM48

*Degradation product

Analysis Code:  LCSU  

Artificial Sweeteners Method 

Sample Prep: Solid-phase extraction               

Instrumentation: Liquid chromatography/tandem mass spectrometry 

Matrix: Water 

OGRL Method Code: LM100 

Bottle Requirements: 4-4oz (125mL) amber glass with Teflon lined caps  

 

Compound/CAS#/Parameter Code     

Acesulfame-K (0.01 µg/L reporting limit)/ 55589-62-3/54209 

Aspartame (0.002 µg/L reporting limit)/ 22839-47-0/54210 

 

Neotame (0.0003 µg/L reporting limit)/ 165450-17-9/54211 

Saccharin (0.02 µg/L reporting limit)/ 81-07-2/54212 

Sucralose (0.1 µg/L reporting limit)/ 56038-13-2/54213 

 

Analysis Code: LCHM_PG

Progestins Method

Sample Prep: Solid-phase extraction              

Instrumentation: Liquid chromatography/tandem mass spectrometry 

Matrix: Water

Reporting Limit: 1 ng/L (except where noted)

OGRL Method Code: LCM96 (except where noted)

Bottle Requirements: 6-4oz (125mL) amber glass with Teflon lined caps or 1-1 Liter amber glass bottle with Teflon lined cap.

 

 

Compound Name/ CAS#: Parameter Code    

Desogestrel (10 ng/L)/ 54024-55-5: 53535, Method Code: LCM97

Drospirenone (10 ng/L)/ 67392-87-4: 53536, Method Code: LCM97

Gestodene/ 60282-87-3: 53537

Levonorgestrel/ 797-63-7: 53538

Medroxyprogesterone/ 520-85-4: 53539

 

Melengestrol acetate/ 2919-66-6: 53540

Nestorone/ 7759-35-5: 53541

19-Norethindrone/ 68-22-4: 53543

Norgestimate/ 35189-28-7: 53544

Progesterone/ 57-83-0: 64523

 

 

Analysis Code:  LCHM2

Estrogens, Androgens, & Conjugates Method

Sample Prep: Solid-phase extraction              

Instrumentation: Liquid chromatography/tandem mass spectrometry 

Matrix: Water

Reporting Limit: 1 ng/L (except where noted)

OGRL Method Code: LCM96 

Bottle Requirements: 6-4oz (125mL) amber glass with Teflon lined caps or 1-1 Liter amber glass bottle with Teflon lined cap.

Compound Name/ CAS#: Parameter Code    

Estrogens

Trans-diethylstilbestrol/ 56-53-1: 64516

17α-Estradiol (17αE2)/ 57-91-0: 64508

17β-Estradiol (17βE2)/ 50-28-2: 64510

Estriol (E3)/ 50-27-1: 64520

Estrone (E1)/ 53-16-7: 64521

17α-Ethynylestradiol (EE2)/ 57-63-6: 64509

Equilenin/ 517-09-9: 64518

Equilin/ 474-86-2: 64519

 

Androgens

Androstenedione/ 63-05-8: 64513

5α-Dihydrotestosterone/ 521-18-6: 53517

Epitestosterone/481-30-1: 64517

11-Ketotestosterone/ 564-35-2: 64507

Testosterone/ 58-22-0: 64545

Trenbolone/ 10161-33-8: 64526

Trenbolone acetate / 10161-34-9: 53518

 

Conjugates   

Androsterone glucuronide/ 1852-43-3: 53519

Trans-diethylstilbestrol glucuronide/ 2408-40-4: 53520   

17β-Estradiol-glucuronide/ 1806-98-0: 53521

Estriol-3-glucuronide/ 2479-91-6: 53522

Estrone glucuronide/ 2479-90-5: 53523

Ethynylestradiol-3-glucuronide/ 60134-76-1: 53524

Testosterone glucuronide/1180-25-2: 53515

Androsterone sulfate/ 2479-86-9: 53525

Equilenin sulfate/ 16680-48-1: 53526

Equilin sulfate/27540-07-4: 53527

17β-Estradiol-3-sulfate/ 481-96-9: 53528

17β-Estradiol-17-sulfate/ 3233-69-0: 53529

Estriol-3-sulfate/ 481-95-8: 53530

Estriol-17-sulfate/ 42028-21-7: 53531

Estrone-3-sulfate/ 481-97-0: 53532

Ethynylestradiol-3-sulfate/ 24560-70-1: 53533

Testosterone sulfate/ 651-45-6: 53534

 

 

Analysis Code:  LCHM_MTox

Sample Prep: Solid-phase extraction              

Instrumentation: Liquid chromatography/tandem mass spectrometry 

Matrix: Water

Reporting Limit: 1 ng/L (except where noted)

OGRL Method Code: LCM96 

Bottle Requirements: 6-4oz (125mL) amber glass with Teflon lined caps or 1-1 Liter amber glass bottle with Teflon lined cap.

 

Compound Name/ CAS#: Parameter Code                            

Beauvericin (2 ng/L)/ 26048-05-5: 53551

Deoxynivalenol (2 ng/L)/ 51481-10-8: 53552

Nivalenol (2 ng/L)/ 23282-20-4: 53553

Verrucarin A/ 3148-09-02: 53554

 

α-Zearalanol/ 26538-44-3: 53555

α-Zearalenol/ 36455-72-8: 53556

β-Zearalenol/ 71030-11-0: 53557

Zearalenone/ 17924-92-4: 53558

 

 

Analysis Code:  LCHM_PE

Phytoestrogens Method

Sample Prep: Solid-phase extraction              

Instrumentation: Liquid chromatography/tandem mass spectrometry 

Matrix: Water

Reporting Limit: 1 ng/L 

OGRL Method Code: LCM96 

Bottle Requirements: 6-4oz (125mL) amber glass with Teflon lined caps or 1-1 Liter amber glass bottle with Teflon lined cap.

 

Compound Name/ CAS#: Parameter Code    

Biochanin A/ 491-80-5: 53545

Coumestrol/ 479-13-0: 53546

Daidzein/ 486-66-8: 53547 

 

Equol/ 531-95-3: 53548

Formononetin/ 485-72-3: 53549

Genistein/ 446-72-0: 53550

 

EOC Custom Request Research Methods: For additional information contact Rachael Lane, rflane@usgs.gov, 785-760-4540. 

Analysis Code: LCPH

Pharmaceutical Method (other compounds available by request)

Sample Prep: To be determined.

Instrumentation: Liquid chromatography/tandem mass spectrometry

Matrix: Water             

Compound Names:     

Abacavir

Acetaminophen

Acyclovir

Albuterol

Amphetamine

Atenolol

Atrazine

Bupropion

Butalbital

Caffeine

Carbamazepine

Carisoprodol

Cefalexin

Cimetidine

Citalopram

Clonidine 

Codeine

Cotinine

Dehydronifedipine

Desloratadine

Desmethyldiltiazem

 

Desvenlafaxine

Dextromethorphan

Diazepam

Diclofenac

Diltiazem

Dimethylxanthine

Diphenhydramine

Erythromycin

Erythromycin-H2O

Famotidine

Fenofibrate

Fexofenadine

Fluconazole

Fluoxetine       

Fluticasone propionate

Gabapentin

Gemfibrozil 

Glyburide

Guanylurea

Hydrochlorothiazide

 

Hydrocortisone

Hydroxybuproprion

Lamivudine

Lamotrigine

Lidocaine

Loratadine

Meprobamate

Metformin

Methadone

Methocarbamol

Methylbenzotriazole

Metoprolol

Morphine

Nadolol

N-desmethylcitalopram

Nicotine

Norsertraline

Nortramadol

Norverapamil

Oxcarbazepine

Oxycodone

 

Penciclovir

Pentoxifylline

Piperonyl butoxide

Propranolol

Pseudoephedrine/Ephedrine

Ractopamine

Ranitidine

Sertraline

Sitagliptin

Sulfamethoxazole

Tamoxifen 

Temazepam

Theophylline

Thiabendazole

Tiotropium

Topiramate

Tramadol

Triamterene

Trimethoprim

Venlafaxine

Verapamil

 

Analysis Code:  LCTS

Solid Method

Sample Prep: Energized Dispersive Guided Extraction and Solid-phase extraction             

Instrumentation: Liquid chromatography/tandem mass spectrometry 

Matrix: Sediments and Soils

Reporting Limit: 

OGRL Method Code: Not Assigned Yet

 

Compound/CAS#: 

6PPD-quinone / 2754428-18-5

6PPD/ 793-24-8

Other tire-related compounds available by request

 

Analysis Code:  LCGS

Solid Glyphosate, AMPA, and Glufosinate Method 

Sample Prep: Derivatization (FMOC)            

Instrumentation: Liquid chromatography/tandem mass spectrometry

Matrix: Solids

Reporting Limit: 1-10 µg/kg 

OGRL Method Code: LCM69

 

Compound Name/ CAS#, Parameter Code (Dry Weight)

Glyphosate/ 1071-83-6: 52168

*Aminomethylphosphonic Acid (AMPA)/ 1066-51-9: 52169Glufosinate/ 51276-47-2: 52170

*Degradation product

 

 

 

Analysis Code:  LCAS

Solid Four Class Antibiotic Method

Sample Prep: Pressurized liquid extraction, Solid-phase extraction

Instrumentation: Liquid chromatography/tandem mass spectrometry

Matrix: Solids 

 

FluoroquinolinesMacrolidesSulfonamides
Ciprofloxacin AzithromycinSulfachloropyridazine
Enrofloxacin ErythromycinSulfadiazine 
Lomefloxacin *Erythromycin-H2OSulfadimethoxine 
Norfloxacin Roxithromycin Sulfamethoxazol
Ofloxacin Tylosin Sulfamethazine 
Sarafloxacin VirginiamycinSulfathiazole 
   
Tetracyclines  -PharmaceuticalsOthers

Chlorotetracycline

*Epi-chlorotetracycline

*Epi-iso-chlorotetracycline

*Iso-chlorotetracycline

Carbamazepine 

Ibuprofen

Chloramphenicol 

Lincomycin

Ormetoprim

Trimethoprim

Oxytetracycline 

*Epi-oxytetracycline

  

Tetracycline 

*Epi-tetracycline

  
Doxycycline  

 

Analysis Code:  LCHS2

Solid Estrogens, Androgens, & Conjugates Method

Sample Prep: Pressurized liquid extraction, Solid-phase extraction              

Instrumentation: Liquid chromatography/tandem mass spectrometry 

Matrix: Solids

OGRL Method Code: Not assigned yet 

Compound Name/ CAS#: Parameter Codes not assigned yet            

Estrogens

Trans-diethylstilbestrol/ 56-53-1

17α-Estradiol (17αE2)/ 57-91-0

17β-Estradiol (17βE2)/ 50-28-2

Estriol (E3)/ 50-27-1

Estrone (E1)/ 53-16-7

17α-Ethinylestradiol (EE2)/ 57-63-6

Equilenin/ 517-09-9

Equilin/ 474-86-2

 

Androgens

Androstenedione/ 63-05-8

5α-Dihydrotestosterone/ 521-18-6

Epitestosterone/ 481-30

11-Ketotestosterone/ 564-35-2

Testosterone/ 58-22-0

Trenbolone/ 10161-33-8

Trenbolone acetate/ 10161-34-9

 

Conjugates   

Androsterone glucuronide/ 1852-43-3

Trans-diethylstilbestrol glucuronide/ 2408-40-4   

17β-estradiol-glucuronide/ 1806-98-0

Estriol-3-glucuronide/ 2479-91-6

Estrone glucuronide/ 2479-90-5

Ethynylestradiol-3-glucuronide/ 60134-76-1

Testosterone glucuronide/ 118-25-2

Androsterone sulfate/ 2479-86-9

Equilenin sulfate/ 16680-48-1

Equilin sulfate/ 16680-47-0

17β-estradiol-3-sulfate/ 481-96-9

17β-estradiol-17-sulfate/ 3233-69-0

Estriol-3-sulfate/ 481-95-8

Estriol-17-sulfate/ 42028-21-7

Estrone-3-sulfate/ 481-97-0

Ethynylestradiol-3-sulfate/ 24560-70-1

Testosterone sulfate/ 651-45-6

 

 

 

Analysis Code:  LCHS_PE

Solid Phytoestrogens Method

Sample Prep: Pressurized liquid extraction, Solid-phase extraction              

Instrumentation: Liquid chromatography/tandem mass spectrometry 

Matrix: Solids

OGRL Method Code: Not Assigned Yet 

 

Compound Name/ CAS#: Parameter Codes not assigned yet            

Biochanin A/ 491-80-5

Coumestrol/ 479-13-0

Daidzein/ 486-66-8

 

Equol/ 531-95-3

Formononetin/ 485-72-3

Genistein/ 446-72-0

 

 

Analysis Code:  LCHS_PG

Solid Progestins Method

Sample Prep: Pressurized liquid extraction, Solid-phase extraction              

Instrumentation: Liquid chromatography/tandem mass spectrometry 

Matrix: Solids

OGRL Method Code: Not Assigned Yet 

 

Compound Name/ CAS#: Parameter Codes not assigned yet            

Desogestrel/ 54024-55-5

Drospirenone/ 67392-87-4

Gestodene/ 60282-87-3

Levonorgestrel/ 797-63-7

Medroxyprogesterone/ 520-85-4

 

Melengestrol acetate/ 2919-66-6

Nestorone/ 7759-35-5

19-Norethindrone/ 62-88-4

Norgestimate/ 35189-28-7

Progesterone/ 57-83-0

 

 

 

Analysis Code:  LCHS_MTox

Solid Mycotoxin Method

Sample Prep: Pressurized liquid extraction, Solid-phase extraction              

Instrumentation: Liquid chromatography/tandem mass spectrometry 

Matrix: Solids

OGRL Method Code: Not Assigned Yet 

 

 

Compound Name/ CAS#: Parameter Codes not assigned yet                                    

Beauvericin/ 26048-05-5

Deoxynivalenol/ 51481-10-8

Nivalenol/ 23282-20-4

Verrucarin A/ 3148-09-02

 

α-Zearalanol/ 26538-44-3

α-Zearalenol/ 36455-72-8

β-Zearalenol/ 71030-11-0

Zearalenone/ 17924-92-4

 

 

Psychoactive Compounds, Preliminary Method Development 

Sample Prep: To be determined.

Instrumentation: Liquid chromatography/tandem mass spectrometry

Matrix: Water                         

Price Per Sample: To be determined.

 

Potential Compounds:

Amphetamines

Amphetamine

Cathinone

Cocaine

*Benzoylecgonine

*Cocaethylene

*Ecgonine Methyl Ester

MDA

MDEA

MDMA

Methamphetamine

Phentermine

 

 

Benzodiazepines

Alprazolam

Chlordiazepoxide

Clonazepam

Diazepam

Estazolam

Flunitrazepam

Lorazepam

Midazolam

Nitrazepam

Oxazepam

Temazepam

Zolpidem

 

 

Barbiturates

Amobarbital

Butalbital

Pentobarbital

Phenobarbital

Secobarbital

 

Hallucinogens

Ketamine

*Norketamine

LSD

*2-Oxo-3-hydroxy-LSD

Methoxetamine

Opioids

Buprenorphine

*Norbuprenorphine Glucuronide

Codeine

Fentanyl

Heroin

Hydrocodone

Hydromorphone

Mephedrone

Methadone

*EDDP

*EMDP

Morphine

Naloxone

Oxycodone

Oxymorphone

Tramadol

 

Cannabinoids, Preliminary Method Development

Research Method for Cannabis Compounds

Sample Prep: To be determined.

Instrumentation: Liquid chromatography/tandem mass spectrometry

Matrix: Water                         

Price Per Sample: To be determined.

Potential Compounds:

Cannabidiol

Cannabinol

Tetrahydrocannabinol (THC)

11-Hydroxy-THC

11-Nor-9-Carboxy-THC

 

Algal and Environmental Toxins (AET) Unit

For additional information contact Zach Laughrey 785-832-3585, zlaughrey@usgs.gov

*All internal Quality Control data must be requested during the establishment of the sample processing agreement or additional fees may apply. 

 

*Call to discuss analysis of Protein Phosphatase 2a Inhibition (785) 764-1408

 

ELISA techniques

 

OGRL Method Name: Description, Parameter Code, Method Code

Microcystin: CAS# 101043-37-2

IMNT2: Total Analysis, 89011, IMM26

IMNT2S: Total High Salinity, 89011, IMM28

IMND2: Dissolved Analysis, 89012, IMM27

IMND2S: Dissolved High Salinity, 89012, IMM29

 

Cylindrospermopsin: CAS# 143545-90-8

IMYT: Total Analysis, 89005, IMM10

IMYTS: Total High Salinity, 89005, IMM20

IMYD: Dissolved Analysis, 89006, IMM11

IMYDS: Dissolved High Salinity, 89006, IMM21

 

Saxitoxin/ 35523-89-8

IMXT: Total Analysis, 89003, IMM08

IMXTS: Total High Salinity, 89003, IMM22

IMXD: Dissolved Analysis, 89004, IMM09

IMXDS: Dissolved High Salinity, 89004, IMM23

 

Anatoxin-a/ 64285-06-9

IMAAT: Total Analysis, 53954, IMM24

IMAAD: Dissolved Analysis, 53955, IMM25

 

 

Algal Toxins by Liquid chromatography/tandem mass spectrometry

 

LCTXO-MT-QT (Marine Toxins only: Total Analysis)

Sample Prep: Freeze/thaw x 3 then filter

Instrumentation: Liquid chromatography/High Resolution Mass Spectrometry via Orbitrap

Matrix: Water

Reporting Limit: 0.10µg/L (except where noted)

OGRL Method Code: LCM87

 

Compound Name/ CAS#: Parameter Code 

13-Desmethyl spirolide C (0.08 µg/L)/ 334974-07-1: 53973

Azaspiracid-1/ 214899-21-5: 53969

Dinophysistoxin-1 (0.30 µg/L)/ 81720-10-7: 53970

Dinophysistoxin-2/ N/A: 53974

Domoic Acid (0.08 µg/L)/ 14277-97-5: 52687

Gymnodimine/ 173792-58-0: 53971

Nodularin R (NDLR)/ 118399-22-7: 52696

Okadaic Acid/ 78111-17-8: 52697

Pectenotoxin-2/ 97564-91-5: 53972

 

 

LCTXO-MD-QT (Marine Toxins only: Dissolved Analysis)

Sample Prep: Filtered 

Instrumentation: Liquid chromatography/High Resolution Mass Spectrometry via Orbitrap Matrix: Water

Reporting Limit: 0.10µg/L (except where noted)

OGRL Method Code: LCM87 

 

Compound Name/ CAS#: Parameter Code 

13-Desmethyl spirolide C (0.08 µg/L)/ 334974-07-1: 53979

Azaspiracid-1/ 214899-21-5: 53975

Dinophysistoxin-1 (0.30 µg/L)/ 81720-10-7: 53976

Dinophysistoxin-2/ N/A: 53980

Domoic Acid (0.08 µg/L)/ 14277-97-5: 65193

Gymnodimine 173792-58-0: 53977

Nodularin R (NDLR)/ 118399-22-7: 56189

Okadaic Acid/ 78111-17-8: 52164

Pectenotoxin-2/ 97564-91-5: 53978

 

 

LCTXO-CT-QT (Freshwater Toxins only: Total Analysis)

Sample Prep: Freeze/thaw x 3 then filter

Instrumentation: Liquid chromatography/High Resolution Mass Spectrometry via Orbitrap

Matrix: Water

Reporting Limit: 0.10µg/L (except where noted)

OGRL Method Code: LCM87

 

Compound Name/ CAS#: Parameter Code 

 

Anatoxin-a (ANTA) (0.08 µg/L)/ 64285-06-9: 68287

Cylindrospermopsin (CYLS)/ 143545-90-8: 52686

Microcystin HtYR (MCHtYR)/ N/A: 52690

Microcystin HiLR (MCHiLR)/ N/A: 52836

Microcystin LA (MCLA)/ 96180-79-9: 52688

Microcystin LF (MCLF)/ 154037-70-4: 52694

Microcystin LR (MCLR)/ 101043-37-2: 63686

 

Microcystin LW (MCLW)/ 111755-37-4: 52685

Microcystin LY (MCLY)/ 123304-10-9: 52689

Microcystin RR (MCRR) (0.08 µg/L)/ 111755-37-4: 52695

Microcystin YR (MCYR)/ 101043-37-2: 52693

Nodularin R (NDLR)/ 118399-22-7: 52696

 

LCTXO-CD-QT (Freshwater Toxins only: Dissolved Analysis)

Sample Prep: Filtered

Instrumentation: Liquid chromatography/High Resolution Mass Spectrometry via Orbitrap

Matrix: Water

Reporting Limit: 0.10µg/L (except where noted)

OGRL Method Code: LCM87

 

Compound Name/ CAS#: Parameter Code 

 

Anatoxin-a (ANTA) (0.08 µg/L)/ 64285-06-9: 65191

Cylindrospermopsin (CYLS)/ 143545-90-8: 65190

Microcystin HtYR (MCHtYR)/ N/A: 52161

Microcystin HiLR (MCHiLR)/ N/A: 52165

Microcystin LA (MCLA)/ 96180-79-9: 65188

Microcystin LF (MCLF)/ 154037-70-4: 65186

Microcystin LR (MCLR)/ 101043-37-2: 63685

 

Microcystin LW (MCLW)/ 111755-37-4: 65185

Microcystin LY (MCLY)/ 123304-10-9: 52163

Microcystin RR (MCRR) (0.08 µg/L)/ 111755-37-4: 64048

Microcystin YR (MCYR)/ 101043-37-2: 65187

Nodularin R (NDLR)/ 118399-22-7: 65189

 

LCTXO-AT-QT (Freshwater and Marine Toxins: Total Analysis)

Sample Prep: Freeze/thaw x 3 then filter

Instrumentation: Liquid chromatography/High Resolution Mass Spectrometry via Orbitrap

Matrix: Water

Reporting Limit: 0.10µg/L (except where noted)

OGRL Method Code: LCM87

Compound Name/ CAS#: Parameter Code 

13-Desmethyl spirolide C/ 334974-07-1: 53973

Anatoxin-a (ANTA) (0.08 µg/L)/ 64285-06-9: 68287

Azaspiracid-1/ 214899-21-5: 53969

Cylindrospermopsin (CYLS)/ 143545-90-8: 52686

Dinophysistoxin-1/ 81720-10-7: 53970

Dinophysistoxin-2/ N/A: 53974

Domoic Acid/ 14277-97-5: 52687

Gymnodimine/ 173792-58-0: 53971

Microcystin HtYR (MCHtYR)/ N/A: 52690

Microcystin HiLR (MCHiLR)/ N/A: 52836

Microcystin LA (MCLA)/ 96180-79-9: 52688

Microcystin LF (MCLF)/ 154037-70-4: 52694

 

Microcystin LR (MCLR)/ 101043-37-2: 63686

Microcystin LW (MCLW)/ 111755-37-4: 52685

Microcystin LY (MCLY)/ 123304-10-9: 52689

Microcystin RR (MCRR) (0.08 µg/L)/ 111755-37-4: 52695

Microcystin YR (MCYR)/ 101043-37-2: 52693

Nodularin R (NDLR)/ 118399-22-7: 52696 

Okadaic Acid/ 78111-17-8: 52697

Pectenotoxin-2/ 97564-91-5: 53972

 

 

 

LCTXO-AD-QT (Freshwater and Marine Toxins: Dissolved Analysis)

Sample Prep: Filtered

Instrumentation: Liquid chromatography/High Resolution Mass Spectrometry via Orbitrap

Matrix: Water

Reporting Limit: 0.10µg/L (except where noted)

OGRL Method Code: LCM87

Compound Name/ CAS#: Parameter Code 

 

13-Desmethyl spirolide C/ 334974-07-1: 53979

Anatoxin-a (ANTA) (0.08 µg/L)/ 64285-06-9: 65191

Azaspiracid-1/ 214899-21-5: 53975

Cylindrospermopsin (CYLS)/ 143545-90-8: 65190

Dinophysistoxin-1/ 81720-10-7: 53976

Dinophysistoxin-2/ N/A: 53980

Domoic Acid/ 14277-97-5: 65193

Gymnodimine/ 173792-58-0: 53977

Microcystin HtYR (MCHtYR)/ N/A: 52161

Microcystin HiLR (MCHiLR)/ N/A: 52165

Microcystin LA (MCLA)/ 96180-79-9: 65188

Microcystin LF (MCLF)/ 154037-70-4: 65186

Microcystin LR (MCLR)/ 101043-37-2: 63685

Microcystin LW (MCLW)/ 111755-37-4: 65185

Microcystin LY (MCLY)/ 123304-10-9: 52163

Microcystin RR (MCRR) (0.08 µg/L)/ 111755-37-4: 64048

Microcystin YR (MCYR)/ 101043-37-2: 65187

Nodularin R (NDLR)/ 118399-22-7: 65189

Okadaic Acid/ 78111-17-8: 52164

Pectenotoxin-2/ 97564-91-5: 53978

 

 

 

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