The age and source of the late Pleistocene Roxana Silt in the Mississippi Valley have been studied since the middle 1800s. Published age and paleoenvironmental data for the Roxana Silt in the Mississippi Valley show that deposition occurred from late marine isotope stage 5 (MIS5) through late marine isotope stage 3 (MIS3) (80–30 kilo-annum [ka]), when the warm to hot interglacial climate of early to middle MIS5 (about 130 to about 80 ka) was transitioning to a considerably cooler and wetter climate. Scanning electron microscopy/energy dispersive X-ray (SEM/EDS) analysis of silt and sand grains from the Roxana Silt exposed in an abandoned borrow pit near Phillips Bayou, Arkansas, was performed as part of a 1990s study of late middle and late Pleistocene loess in the unglaciated lower Mississippi Valley. Results from that study were summarized in 1990s publications, but the data for sand and silt grain morphology and mineralogy were not published. Some of the SEM/EDS analyses of the Roxana Silt from that late 1990s study are presented in this report. Combined with previously published chronostratigraphic and pedostratigraphic data for the Roxana Silt at Phillips Bayou, the SEM/EDS data indicate some degree of syndepositional weathering and pedogenic alteration during and after gradual eolian deposition in late marine isotope stage 4 (MIS4) and MIS3 (about 60 to about 30 ka). Results from the SEM/EDS analyses support previously published paleoclimate interpretations indicating that at least as far south as northern Mississippi, the climate of the Mississippi Valley in MIS4 and MIS3 (about 70 to about 30 ka) was cool to cold and humid to wet.
