A dithizone method for the determination of lead in monazite
In determining lead in monazite [(Ce,La,Th)PO4]--to be used as the basis for geologic age measurements--it was necessary to eliminate interferences due to the presences of phosphates of thorium and the rare-earth metals.
The method, in which monazite samples are attacked with hot concentrated sulfuric acid, taken up with dilute nitric acid, lead extracted as the dithizonate and then determined spectrophotometrically at 520 mμ, was successfully applied to a series of monazite samples. Rapid determinations were made with good reproducibility.
Citation Information
Publication Year | 1956 |
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Title | A dithizone method for the determination of lead in monazite |
DOI | 10.3133/tei630 |
Authors | R. A. Powell, C. A. Kinser |
Publication Type | Report |
Publication Subtype | USGS Numbered Series |
Series Title | Trace Elements Investigations |
Series Number | 630 |
Index ID | tei630 |
Record Source | USGS Publications Warehouse |