The U.S. Geological Survey (USGS), in cooperation with the U.S. Air Force Civil Engineer Center (USAF/CEC), conducted a pilot study at Malmstrom Air Force Base (MAFB) to evaluate the utility of two non-invasive geophysical techniques for detecting hydrocarbons in subsurface materials. Electrical resistivity tomography (ERT) and electromagnetic induction (EMI) surveys were completed August 28–29, 2023, along 7 transects overtop contaminated and uncontaminated sites for comparison. Additionally, the USGS completed ultraviolet optical scanning tool (UVOST) soundings and collected soil samples from temporary boreholes to validate geophysical survey results. A total of 11 UVOST soundings and 7 boreholes were completed August 28–31, 2023. Two soil samples from various depths were collected from each borehole for a total of 14 samples. Ten quality assurance/quality control samples consisting of 2 field equipment blanks (1 per day), 4 replicate soil samples (2 per day), and 4 trip blanks (2 per day). Soils were tested for volatile organic compounds, semi-volatile organic compounds, gasoline range organics, diesel range organics, metals, and per- and polyfluorinated substances (PFAS/PFOA).