Energy Resources Program
Data and Tools
Investigating the effects of broad ion beam milling to sedimentary organic matter
To test if reflectance increases to sedimentary organic matter (vitrinite) caused by broad ion beam (BIB) milling were related to molecular aromatization and condensation, we used Raman and Fourier transform infrared (FTIR) spectroscopies to evaluate potential compositional changes in the same vitrinite locations pre- and post-BIB milling. The same locations also were examined by at
Chemistry Data from Southern Florida Canals Collected in Support of the Aquatic Cycling of Mercury in the Everglades Project
Several canals in southern Florida run from Lake Okeechobee through the Everglades Agricultural Area (EAA) and feed water to the northern Everglades. Agricultural and water-management practices affect the water quality of these canals. Fertilizers added in the EAA flow into the canals and are transported to treatment areas which remove much of the phosphorous in the water, but are not as
U-Pb ages of detrital zircons in Paleogene strata of the Gulf Coast
This data release contains 60 detrital zircon age spectra, based on U and Pb isotope ratio measurements for 9399 single grains. The samples are from Paleogene strata of the U.S. Gulf Coast. Of the 9399 single grain measurements, we recommend that 8640 yield ages that are suitable for construction of detrital zircon age spectra. Comments tagged to individual grains explain the reasoning for ex...
Fluorescence spectroscopy of ancient sedimentary organic matter via confocal laser scanning microscopy (CLSM)
Fluorescence spectroscopy via confocal laser scanning microscopy (CLSM) was used to analyze ancient sedimentary organic matter, including Tasmanites microfossils in Devonian shale and Gloecapsomorpha prisca (G. prisca) in Ordovician kukersite from North American basins. We examined fluorescence emission as a function of excitation laser wavelength, sample orientation, and with respe
ATR data from interaction of kerogen with brine-saturated supercritical carbon dioxide (CO2) and its implications to geologic carbon sequestration and enhanced oil/gas recovery (2018)
The dataset covers Attenuated Total Reflectance (ATR) measurements taken from altered kerogen in shales from the Woodford formation. The ATR measurements were taken after the samples were run through supercritical CO2 alteration experiments in a brine solution.
Organic Petrography and Diagenesis of Leonardian Mudrocks and Carbonates, Midland Basin, Texas (2018)
As part of a larger study, organic petrographic features of Leonardian Wolfcamp A repetitive siliceous and calcareous mudrock and fine-grained carbonate lithofacies cycles occurring in the R. Ricker #1 core from Reagan County, Midland Basin, Texas were evaluated. The objectives of the petrographic investigation were to estimate thermal maturity, identify organic matter types and abundan
Subsurface stratigraphic picks of the Middle–Upper Triassic Shublik Formation, Alaska North Slope
The Middle–Upper Triassic Shublik Formation is the main source rock for Arctic Alaska oil and gas accumulations, including the supergiant Prudhoe Bay field. A revised stratigraphic framework recently has been developed in outcrop for the Shublik and related strata that delineates three large-scale stratigraphic units: 1) the lower clastic (LC) unit, 2) the middle carbonate-
Sample mounting for organic petrology: no thermal effects from transient exposure to elevated temperatures (2019)
For sample mounting, organic petrology laboratories typically use cold-setting epoxy-resin (e.g., 40°C, used by Oklahoma Geological Survey, OGS) or heat-setting plastic (e.g., 180°C, used by U.S. Geological Survey, USGS). Previous workers have suggested a systematic vitrinite reflectance (VRo) increase was associated with the thermoplastic preparation process%2
Oil-source rock correlation studies in the unconventional Upper Cretaceous Tuscaloosa marine shale petroleum system, Mississippi and Louisiana, USA (2019)
The U.S. Geological Survey assessed undiscovered unconventional hydrocarbon resources reservoired in the Upper Cretaceous Tuscaloosa marine shale (TMS) of southern Mississippi and adjacent Louisiana in 2018. As part of the assessment, oil- source rock correlations were examined in the study area where operators produce light (38-45° API), sweet oil from horizontal, hydraulicall
Direct Trace Element Determination in Oil and Gas Produced Waters with Inductively Coupled Plasma – Optical Emission Spectrometry (ICP-OES): Advantages of High Salinity Tolerance (2019)
Waters co-produced during petroleum extraction are the largest waste stream from oil and gas development. Reuse or disposal of these waters is difficult due both to their high salinities, which can greatly exceed 35 g/L (seawater equivalent), and also the sheer volume of wastewater generated, which is estimated at nearly 900 billion gallons per year across the United States. Beyond di
Organic Analysis of Oilfield Produced Water from the Williston Basin, North Dakota
The organic composition of produced waters (flowback and formation waters) from the Bakken Formation and the Three Forks Formation in the Williston Basin, North Dakota were examined in this study in order to aid in the remediation of surface contamination due to spills during transport and help develop treatment methods for recycling. Twelve produced water samples were collected from wells
Testing reproducibility of vitrinite and solid bitumen reflectance measurements in North American unconventional petroleum systems (2019)
To test reproducibility of vitrinite and solid bitumen reflectance measurements in mudrocks, an interlaboratory study (ILS) was conducted using six samples from United States unconventional petroleum systems. Samples selected from the Marcellus, Haynesville, Eagle Ford, Barnett, Bakken and Woodford are representative of resource plays currently under exploitation in North America. A